Qualification package · diffraction · tomography · certification

Measured, refined, certified.

FusionCert is the qualification package for fusion first-wall materials: a specimen registry, a diffraction and tomography analysis suite built on GSAS-II and scikit-image, and a certificate engine that issues only on recorded evidence. One system from raw frame to signed certificate.

RietveldGSAS-II engine
5 toolsanalysis suite
13grades under test
SHA-256on every raw frame
Analysis suite

The refinement is inside, not in another window

Upload the pattern, the instrument file and the phases, and the refinement runs in the registry with the result bound to the specimen. The engines are the ones the community already trusts.

Rietveld · Le Bail
GSAS-II refinement

Staged refinement of background, cell, isotropic size and microstrain and sample displacement, with GSAS-II's own estimated standard deviations, Rwp and goodness of fit. The same powder mathematics as TOPAS and FullProf, scriptable and auditable.

Peak broadening
Line-profile analysis

Williamson-Hall and modified Williamson-Hall with contrast factors, instrument correction from the standard, domain size, microstrain and dislocation density by Williamson-Smallman and Wilkens.

Stress
sin²ψ and depth profiles

Biaxial residual stress with hkl-specific elastic constants and d₀ solved rather than assumed; lattice-strain depth profiles in ppm from edge-on and taper-section scans.

Tomography
Threshold and watershed segmentation

Otsu or fixed threshold, distance-transform watershed to separate touching pores, porosity, pore-size distribution, largest pore and crack-like count, the Avizo chain on scikit-image.

Provenance
Every result traceable

The input file is hashed, the method and its parameters are stored with the numbers, and the fit quality sits beside each value in the record and on the certificate.

Scale
Workstation worker

The same code runs on the beamline workstation for full tomograms and batch refinements, submitting through the API with identical provenance.

From lot to certificate

One unbroken chain of evidence

A result that cannot be traced to a specimen, a protocol and a raw file is an anecdote. The registry refuses to issue a certificate without all three.

01
Lot receivedSupplier, batch reference and certificate of analysis hashed on arrival.
02
Specimen registeredPersistent identifier, QR label, cut lineage and pristine or implanted twin.
03
PreparedPolishing and mounting events logged against the SOP in force.
04
MeasuredDiffraction and tomography bound to protocol, calibrant, energy and raw-data hash.
05
RefinedGSAS-II lattice parameters, line-profile and stress analysis with stated uncertainty.
06
EvaluatedPredicates checked on recorded data only. Missing data fails.
07
CertifiedFrozen evaluation, hashed serial, public verification page.
Instrument

Built around the Extreme Conditions Beamline

Baseline and post-irradiation measurements run at P02.2 on PETRA III: transmission and grazing-incidence diffraction, propagation radiography and absorption tomography on the same coupon, with CeO₂ calibration refined once per energy.

42.7 keVtransmission XRD
25.6 keVgrazing incidence
≤ 8 µmGIXRD probe depth
2 to 5 µmedge-on depth step
  • Tungsten, W-K, W-Re, W-Y₂O₃, W-Cr-Y and Wf/W, with Mo, Re, B₄C, SiC and graphite
  • Proton implantation at HZDR as the irradiation surrogate
  • Rietveld and Le Bail refinement in GSAS-II, line-profile dislocation density
  • Threshold and watershed tomography segmentation, porosity and pore statistics
  • Comparative grade baselines with outlier flags beyond three standard deviations
Platform

Qualification infrastructure for fusion materials

Identity
Specimen passports

IFUEL-W-L01-007 and its cut children, each with a QR label that resolves to its own record, paired as pristine and implanted twins from adjacent positions.

Provenance
Protocol-bound measurement

Technique, instrument, energy, calibrant, analysis software and the SHA-256 of the raw frame are stored with every number and its uncertainty.

Acceptance
Predicate-based criteria

Versioned criteria sets evaluate lattice strain, microstrain, porosity and pore size against agreed limits, and refuse to pass on absent data.

Trust
Hash-chained record

Every event is appended to a chain that the dashboard re-verifies on each load; certificates freeze their evidence and can be checked publicly by serial.

Comparison
Grade baselines

One value per specimen builds the envelope for each grade and quantity, so a batch from a new supplier is judged against the whole campaign.

Integration
Analysis worker and API

Results flow from the beamline workstation through a token-authenticated API; CSV export and JSON records for every specimen.

Context

The materials that face the plasma

Inertial fusion
IFuEL and the first wall

Within the BMFTR "Fusion 2040" programme, the IFuEL project assesses candidate first-wall materials under fusion-relevant conditions, from tungsten grades carrying each European mitigation strategy to low-Z ceramics for inertial confinement.

Qualification
Why a registry, not a spreadsheet

Batch-to-batch variation in porosity, texture and inclusions is otherwise mistaken for radiation damage. A pristine baseline measured under one protocol is what makes a post-irradiation shift meaningful.

From the first frame to the signed certificate.

Register a lot, refine the pattern, segment the volume and issue the certificate without leaving the record.

Beamline access
Staff and scientists

Register specimens, record measurements, define criteria and issue certificates.

Enter workspace →
Industry portal
Suppliers and partners

Follow your own lots and download the records and certificates that belong to you.

Open partner view →
Public check
Verify a certificate

Enter a serial to confirm it exists and that its hash is intact, with no data exposed.

Check a serial →